monrfn reflection numbers for monitor standard measurement

taurfn reflection numbers for absorption correction measurement

bkgrfn reflection numbers for background correction measurement

range limits of reflection numbers and angles

NICNAK Option Code

data scan method t2t θ-2θ scan

wyc Wyckoff scan

omg ω scan

number of steps¹ steps n 96

data set number datset m 1

append to bdf append append to existing l. r.refl

noappend create new logical record refl

force RFT typing² rftn set all hkl on file nic

list reflections list n all

τ reflection range taurfn n mdefine τ hkl no. range

1 If the number of steps is specified as zero no step scan information will be written to the output archive bdf.

2 See the description of the Nicolet file and the definition of RFN in the Reference Manual. All reflections on the nic file will be given the value rft=n, where n is 0, 1, 2, or 3 for regular, standard, phi-spin standard, background measurement.

monrfn 1 min reflection number (RFN) to be RFT=1 0

2 max reflection number (RFN) to be RFT=1 32767

taurfn 1 min reflection number (RFN) to be RFT=2 32000

2 max reflection number (RFN) to be RFT=2 32100

bkgrfn 1 min reflection number (RFN) to be RFT=3 -1

2 max reflection number (RFN) to be RFT=3 -1

range 1 min reflection number (RFN) to be accepted 0

2 max reflection number (RFN) to be accepted 32767

3 min 2θ -360

4 max 2θ +360

5 min ω -360

6 max ω +360

7 min φ -360

8 max φ +360

9 min χ -360

10 max χ +360